国产精品边做奶水狂喷无码_亚洲精品中文字幕不卡_国产精无久久久久久久免费_日本精品免费看_国产精品视频播放_国产欧美日韩二区

ZHEJIANG ZANCHENG LIFE SCIENCES LIMITED

浙江贊誠生物科技有限公司

ZHEJIANG ZANCHENG LIFE SCIENCES LIMITED

Specializing in the production and management of intermediates and fine chemicals

1,2-dimethoxyethane

Chemintel Technology

1,2-dimethoxyethane

Information English name: 1,2-dimethoxyethane
CAS Number: 110-71-4
Molecular formula: C4H10O2
Molecular weight: 90.12100
Exact quality: 90.06810
PSA: 18.46000
Physicochemical properties

Appearance and properties: water white liquid
Density: 0.867 g/mL at 25 °C(lit.)
Boiling point: 85 °C(lit.)
Melting point: -69 °C
Flash point: 32 °F
Refractive index: n20/D 1.379(lit.)
Water solubility: Miscible
Stability: Stable, but explosive peroxides may form on exposure to air. Test for the presence of peroxides before heating. Avoid heat, light, air. Highly flammable. Store under inert gas.
Storage conditions: The warehouse is ventilated, low temperature and dry, and stored separately from oxidants.
Vapor density: 3.1 (20 °C, vs air)
Vapor pressure: 187mmHg at 25°C

Production method
1. Derived from the reaction of ethylene glycol monomethyl ether and metal sodium; methyl chloride. Reflux ethylene glycol monomethyl ether and metal sodium together until the metal sodium is completely reacted, and the temperature is lowered to 45° C., and methyl chloride is introduced. After the reaction is completed, fractional distillation is performed to collect the fraction at 84-85.5°C to obtain the finished product. Refining method: The inspection method of peroxide is the same as that of ether. Peroxide can be refluxed with stannous chloride or removed by activated alumina. Then add a small amount of metallic sodium to remove trace amounts of water. Other refining methods include first drying with sodium wire and adding lithium aluminum hydride to distillation under nitrogen flow. It can also be dried with anhydrous calcium chloride for several days, filtered, distilled with sodium metal, or preserved with lithium aluminum hydride, and distilled before use.
2. While stirring, add sodium metal to ethylene glycol monomethyl ether in small amounts at 60°C, and control the temperature at 78-81°C. After the sodium metal is added, cool to 45°C, and then pass in methyl chloride. The reaction formula is: After the reaction is over, distillation is carried out, and the 84.5-85.5°C fraction is collected to obtain ethylene glycol dimethyl ether.
3. After drying with sodium wire, add lithium aluminum hydride for distillation in the presence of nitrogen, or use anhydrous calcium chloride to dry for a few days, filter out the calcium chloride, add sodium metal for distillation, or add lithium aluminum hydride and place it. Now distilled.

Use It is mainly used in the fields of polymer chemistry, electrochemistry, boron chemistry, and also used in organic synthesis solvents such as resin and nitrocellulose.
【BACK】

BACK
TOP

主站蜘蛛池模板: 黄色在线亚洲 | 国产精品民宅偷窥盗摄 | 精品人妻无码一区二区三区下一 | 在线视频免费观看一区 | 亚洲AV最新在线观看网址 | 台湾佬自拍偷区亚洲综合 | 性生大片免费观看高清视频 | 无码人妻精品一区二区三区在线 | 国产一区二区三区AV在线无码观看 | 狠狠躁夜夜躁人人爽天天不卡软件 | 国精产品999香蕉 | 青青青青青国产费线在线观看 | 性欧美长视频免费观看不卡 | 日韩视频精品在线观看 | 人妻少妇精品中文字幕av蜜桃 | 人妻熟女一区二区aⅴ图片 亚洲精品国产一区二区 | 免费无码AV一区二区三区 | www.四虎在线观看 | 91精品一区二区中文字幕 | 亚洲AV最新天堂地址 | 欧美视频在线观看免费观 | 久久人妻天天AV | 无码人妻丝袜在线视频 | 国产成熟妇人高潮A片 | 久久久夜精品 | JIZZ中国JIZZ在线播放 | 亚洲欧美国产成人综合不卡 | 久久夜色撩人精品国产 | 日本天堂免费观看 | 久久无码中文字幕无码 | 成人性做爰aaa片免费看 | 国产xxxxwwww | 亚洲AV无码久久三宫椿系列 | 韩日免费视频 | 按摩高潮A片一区二区三区 久久亚洲精品无码Va白人极品 | 1000部啪啪未满十八勿入不卡 | 亚洲成人在线视频网 | 久久久久国色AV免费观看 | 在线观看成人无码中文av天堂 | 高潮毛片无遮挡免费高清 | 日本欧美国产一区二区三区 |